INEB
INEB
TitleCrystallisation studies of biodegradable CaO-P 2O 5 glass with MgO and TiO 2 for bone regeneration applications
Publication TypeJournal Article
2004
AuthorsDias, AG, Tsuru, K, Hayakawa, S, Lopes, MA, Santos, JD, Osaka, A
JournalGlass TechnologyGlass Technol
Volume45
Issue2
Pagination78 - 79
Date Published2004///
00171050 (ISSN)
Biodegradation, Bone Regeneration, Crystallization, Differential thermal analysis, Diffractometers, Glass ceramics, Glass matrix, Glass transition, Laser diffraction, Lime, Magnesia, methanol, Monochromators, Precipitation (chemical), Temperature scanning, Titanium dioxide, X ray powder diffraction
CaO-P 2O 5 glass ceramics with small additions of MgO and TiO 2 were prepared in the ortho and pyrophosphate regions by powder sintering and crystallisation through heat treatment at different temperatures determined from differential thermal analysis (DTA). The glass ceramics were analysed by x-ray diffraction (XRD) and it was observed that α- and β-Ca 2P 2O 7 were the first phases to precipitate in the parent glass matrix at a temperature of 681°C, followed by CaTi 4(PO 4) 6 and TiP 2O 7 at temperatures between 703 and 725°C. The β-Ca 2P 2O 7 and CaTi 4(PO 4) 6 phases are usually considered as biocompatible and bioactive and, therefore, these glass ceramics seem to show good potential for bone regeneration applications.
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