INEB
INEB
TitleThe effect of slurry preparation methods on biaxial flexural strength of dental porcelain
Publication TypeJournal Article
2011
AuthorsPelaez-Vargas, A, Dussan, JA, Restrepo-Tamayo, LF, Paucar, C, Ferreira, JA, Monteiro, FJ
JournalJournal of Prosthetic DentistryJ. Prosthet. Dent.
Volume105
Issue5
Pagination308 - 314
Date Published2011///
00223913 (ISSN)
article, chemistry, comparative study, Complex Mixtures, Crowns, dental care, Dental Porcelain, Dental Prosthesis Design, Dental Stress Analysis, Dental Veneers, denture, drug mixture, evaluation, materials testing, pliability, tooth crown, tooth prosthesis
Statement of problem. One-step and incremental mixing procedures are currently used to produce dental ceramic pastes. In the ceramic industry, high quality is obtained using one-step mixing, but in dentistry, the best method has not been yet determined. Purpose. The purpose of this study is to evaluate the effects of 2 mixing techniques on the biaxial flexural strength and microstructure of dental porcelain. Material and methods. Feldspathic porcelain discs (2 × 15 mm in diameter) were produced and divided according to the ceramic paste preparation method, powder-liquid incremental mixing group (n=50) or one-step mixing, as a control group (n=50). Specimens were tested for biaxial flexural strength and characterized using porosimetry, relative humidity, SEM/EDS, XRD, and FT-IR analyses. Statistical analysis was conducted using Weibull statistics. The Weibull modulus, characteristic strength and relative humidity were compared between groups, using Student's t-test and Mann-Whitney U test (α=.05). Results. The powder-liquid incremental mixing group showed significantly higher values (SD) of Weibull modulus (6.74 (0.70), P<.001) and characteristic strength (79.87 (2.01) MPa, P<.001) when compared to the one-step mixing group (4.94 (0.94) and 75.95 (2.61) MPa). Significantly lower mean (SD) relative humidity values (P=.009) were found for powder-liquid incremental mixing group (20% (0.5%)) compared to one-step mixing group (22% (1%)). XRD spectra showed that the one-step mixing group produced higher amounts of the amorphous phase. Conclusions. Specimens produced by the incremental mixing technique showed higher biaxial flexural strength than one-step mixing. © 2011 The Editorial Council of the Journal of Prosthetic Dentistry.
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